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=7
=7
\r,
1Ii.{.r
I.7
,
,l ryIlubus
anC .Schem:
of
,
.r4i+sr'
-
'1 oE C.\Lr lrJT
Exan-:-r
at-i.nn of
(utx:cationaj.
frr.{ustrial Chenristry
sub i ect
)
fND'lS!'Rf -rL Ct-Ill4f
SB\. (Voccat rcr7al su.:i cc,: )
There rrvilL Je : v, r:h.:3iy- oaDers ,: .-d tT^/o
Dractical
papers, prrject r^ror i .t'-r.f .ii_vr-vo<.,.e anf -1ntel,ral
assessment.
The orCer .>f DaDers .ilt at.,tn of exanir,;rtion a:rd
marks
a.l-lotted are as f:llc,^:.
o r -.--.
r
tlame of p,rper
fnCustrlal
fndustriai
fndustrlal
fndustrial
hdustrial
fndustrial
Chemistry paper. I First y--qrr
Chemistry Da:re: fI Sr:eonC feap
Clrerni.str\,r .;f,apel T;I Serloirl -ear
Chemistry pap,.5 fV Secon'l year
Chgni.st; v r).roer \f q,a ton I 'er- :
Che.nislry paper \Ir 'Inird 1,'),.rr
Toral for ti:ecrv
3 nrs
3 hrs
3 hfS
3 hrs
3 t, rs
3
'70
60
60
60
60
__ft_
&n^s
38C
PRiCTTC.TLS I
?
Pacer - !.tdustrial anal.zsig secx)nd ve- tr
3 hrs
Paoer Tf Orqanic S.rl_f abu
seeonrl v€ct:. 3i-rr:s
,fhirrj
Nqn. Ugi_v_grq+ly E-xdmiriation
v?rr -, -- j
(rnternal assessment )
Projec! wcrk and viva-voce
- gfrirO rledr
Total _ fo-r ;rrCtpticol
-/occaticnalTotal for
subj ect ( lheor--.r anrl
practica- )
50
50
50
-'70-
220
600
'Pattern cE gg,erqtion
papFrs .aie,i listrlb,tion of mark.s
All question paD3rs irr rheor.;, wiLr_hav,: three sections A,B.. and
C for InCustrial. Che.nlst::y Fa:crs f and \,1
Sectlon .\: 15 questions out of 20 rnarks tc be
'
... answere-l Each 2 ..narks
se,ction B: 4 qr_res'Llons
6
EaCh
5 marl<s
Marks
3p :'
!r
tO }--rc lnsniefed
20
2 questions out cf 4 to 'oc answ:red
eaclf'
1O
'20
marks
Tbtal
'70
rn-rrk.s
rv! rndustrLal Chemj-stry paper iI
Sectj.cn \: 5 questions cut of E to .Jf,e.dnsr/rered
each 2 marks
.
secrion B: i; gy=L=ls.2i of 1Lt5:- \'--
f,
\r
1n
ry
-2-
4l
I
Marks
Section
C:
2 cnrestlon cut of 4 to p-e answered
20
each1O mrrks
Eor
Seceti-on
60
fndustrial ChernistrY PaDers rrr-fv
i\: 15 questions out of 20 to ]re answereC
30
each I merks
t.
20
Section B: 4 question5 out of 6 to be ansnrerel
"a
each 5 marks
'L question out of 2 Lc l>e ansrnrered
Section
10
each 10 m.:rks
60
total ina rks
Distribution of teaching hct-lrs for tneor''r anr-l practic_lls per
week shall be as follows.
Practlcal
Ihsgry
3 hrs
4 hrs
First Year
10 hrs
12 hrs
Second Ye=r
4 hrs''
3 hrs
Third Year
18 hrrs
18 hrs
a
Topic wise Cistr-ibutio: of iil,-.rks cxp3cte,l in the questlon oa,oers
fnd.ustrial Che'nistr-g - l-: I
qery.
[?._?E__!_qr_:hi!E L!_q. rreishtaqe of
marks
fn:ir:strial .\spects
fndustrial trspects
fndustrial- asoects
Pclluticn
Effluent tre.tt'x3nt
of oroan-ic chemir;tr:y
of fncrq.,.rric Chr:mistl'v
cf physj-cel- Chemistr-v
and vr,aste m.tn,gen=nt
Tct:r1
fndustrial Chemis.trv DaDer fI
Material an.1 enerqy balance
Di,emonsions,rnrl Unlts
Ma+-ertal balance r.vithcut Chemicalreaction
Material .baf ence with Chemical re,:ction
Ener,ly balances
.ud EluiC fiow .ud heat
Ulitities
transcort
fnCustrial Chemistry p?-per IfI
M.aterla] Science
Mech'tnical- procerties, \''lr.l:.11-s .,1-,rC
"-. -Io-,'s cement, cerannies
PcI rrner,s, GIa.ss, Cotr,-.ts ,i,J,l
IJnit operati,cns in Chemicil- Tnir.:.str.ir
Di st il-lation,
ibsr:r-":tion, E..--r-16::itron
20
25
20
25
2A
25
L2
15
18
LU
9C
110
3 hrs
5
1l hrs
20
19 hrs
19 hrs
)n
30 hrs
25
-r0
90
l6
15
14
')
,1
20
15
25
Contd. . .3..
\
R
"t
a
r'-,
Ll-
teechinq
hrs.
No. o:E
Fiiri-r.ation, Crvst ellrzation, Extrlction
l{ixj-rq, Drving
\
fndustrial Chemistr-y r)rcer J-/
fndustr-ial Organizat ion
Proc ess instrumentati_on
fnCustrial- -.naLvsis
of
23
25
13
.10
90
90
30
3l
30
30
mark.s
30
Total
fnifustrial- Chemistry paoer V
Chemical process economics
Unit pr.)cesses in Orr-r-tnic Chem-ica1
I,lanuf acture
Nitr-etlon
90
)o
30
30
1a
72
9
10
9
10
7
6
7
6
7.
6
Sulf onati-on
OxiC.tion
I{ydcoze_t:t _ion
Alkylatj_on .enl trsti:rfic:ticn
$l
-feightage
.-rmin--ticn
Hlzdrcl,rrsis
'7
Histcri-6al -:,eckgounrl, :ha:-:-,..sc,IDCCs . ),
Phytcchemical, evel,.1licn, ccnstituti,:i-i
iso-lation quality contrcll
Fornui3tions, Ascept-ic ecCdlr_1crr,
excepients surgic'll dressinqs,
Dackalginq
5
z.z
4
90
l0
1
7
2'7
25
26
Dlff er-ent cI,:sses b,rlk riruqs
ManuJ-'a-cture via frrnentaticn
R{(D activit.Les & Requlatorl.r regurents
72
t2
6
90
J
J!&
che ni.zrr
tz
Nomencl.ttui-e Generic n:lnes, Trade n,:ine.s
Rar,r inateriais for oro'enic compoun.Js : peircr_.un:
I\T''IIural las, Fra-cticnaticn c-rf crudc oiL, crrckinq,
refor-n.inq, hyCrofornin,l, j_scineris,rc j :n.
(l: Hrs)
COlf : T\r:esr strrrcture, :ri-L-r t-r,:ids, .listiIl._ti-_.n
of crr;t1, chemic,els derived therefrtm
Rereweb}.e
nat,rrai rescurces : Cellulos.t, St.,r^ch_
Prcperties, nio-iif ic.tticn
im)ortant 1n,:1. chernic tI.s
deriveri frc'n them, .sfc.lhcl rnd .lcoh.:l_ ,1;ased
chetmical s, ox.rl-1c tcirl , f urfur---I
(t
Hrs
)
3ontd. .4.
.
-4IqCus51-.ri.a1
aspects of horq
Bas:-c rrreral1urqical operrtl-ons
Calcinatiorry. Roas-,.,-6q, Ref injng
Pulverj-zeticn,
(3 Hrs)
f
Physrcochemic.:l prdncir:1es of extri:ction of
Iron, Ccpoer, Leld, Silver, Sodium, -'il-r.rminiurn,
Magnesium, Zinc, Chromj-um
(9 grs)
fncr-ganic materials of irrdustrial import.rnceforms, structure .end
?heir availability,
moCification. rilumina, sil-ica, silj-cates,
c1a','s, mica, carbon, zeoI11-es.
(3 firs)
istry.
lncgptri"t ".pect= of P
Surf rce chemisrry an,i fnterf.cla.l ohenomen,r:
-ldsor-ption isoth,3rnt, -sc1s, Gels, Ernulsj-cns,
Mic:-oemul.sicns, Mj_cel_'l.es, iercsoIs, Effect of
surfactoats, !l.rrlr3irl'-t,:i;
Ccetalrrsis : Intro.luci-" -r T-',:s
Hcrnoleneorts
ana Heteroqeneou.s, tsfsic orinciples, rn--ch.-nisms,
' F.Lctors :f+ectinq the perf.lr''-r-.nce, fntroduc;icn
to phase transfer catalysis, Enzyme "-13lr7ze,i
reactions - R3te model- , Ta,^l'rstrially iniportnnt
reactions
(fg Hr's)
(lO Urs)
BOOKS
CoaI Concersion, E.J. Hoffmann, the Enerqcn co.,
Lavamic, 'nlycminq, Tl .5.-\.
fntroductj-on to petroleum chen.icals, H. Steiner,
perg.-Imcn press
Frcm -"grocarbons to oetrccheinic..ls, L. F. Hetch and
S. Mr€arm, Gul-f Publichinr Co., Hoiiqler.
Cotton-ceIl-ul_ose : Its chernisr-r-r
and ?echrnology, HaIl/ -;,G.
Metho.ls in Carbohydrfte
CeJ.lulcse, rdhistler,
Che-n,
stry,
',,ro1.3,
R. L"
Catal-ysis ir Bcience & i:cru,oL,cqv, .\ndersonJ.
Catttlys .s j-n micelllr
Fen,il::r J. anC Fendler
aa.d
n cromo-Iecular
s\,,stems
E.
ccntd. - 5" .
\
|_,
-_4.
-5in Theorv an.1 pr,1ctice,.
Rideaf , E. K. and Tc1y1or,
Fi. S.
3.rtllysis
"t
::l:;"1:.:."r".
caralysis, principre and
?echniquesl
Surface Chemistry, djJ-*Blker.?Tlann,,lc,.r.Cemic
press.
Physic.:l chemistry of
Surf aces, A. hi. .-:d:mson
Catalysis : Heterogeneous
.end Homoqeneous,
Delmon, Elsevier Science publisher.
Princin.l_es of extreetive
metr-LIurqv,
Herbrshi, VoI 1,2
?hccry of ..net-:llurgical
proeesses,
lro-l-sky A anrl
SerglewsisrrTa, g.
?extbook of met.allurgy,,
Baiky A. R
C]eys, H, Ries, John
wileys and Sons
Thcor\2
)f rn=t:1lurr71ca1 or( lesses
Eillipov, Mi.r publi.cation
Po-l_-Luti.on
'rj.r,
oxl6qen,
,sts,A;&"y"ro,
w,rr r,
.here, Flora anri faunl./ Tnerg.y,
Soif .
Pollutants anC th_-ir
statutcry
polluticn evalujli )n ..nethoCs. limits.
Bj.osp
1ir
J-ution_V:rious
rDo1 lutant s.
water po} luticn_Organic,/inorganic
Noise pollution
(a
Hr-.-.'
(: Hr:
po-l_
(s
icol_-l_,rr:
Hrc l
rnt s"
Sew,.rge ana-l-Itsi s
pesticide pollution
R,rdiation l>ol-l_utj.on, Green
house eff
=cc, Ftlure.
Princip.l-:s an-l equioments
for aerobj.c. anrercbie, (g
trc,ef'Tsn1, adsorDtion,
Hrs)
fj-ltration,
sedimentet-ion.
B,rrr
fi l.ters, elee.trostatic
precipit'1tor,
eliminatorsr wet scrubbers
r-lst
(+ H:-s,
i,bso6536s
So1id waste m.:ln.lqjm:nt
fndustri-r1 saf:ty
(z Hr.,.
(z I-r:.=,
(z .: ,s)
,
Conr_
i-
,
5
)
J
D-
-- g_
-6-
a
BOOKS
Pollution control in chemieal .1od a11ied jndustries,
Mahajan S.P.
Poll-ution control in industries.
by Jones H.R.
i\ serles of books
System's .\ppro.-r.ch to fj-r Pollution Control,
R.J. Bibbero and f .G. Young
.:tir Pollution-Vo1-f-fv Editor, ,-r. C Stern,
.\cademic Press, NBw YoYrk
casl Purification Process for Air Pollution. control,
G. Nonhebel Newnes-Butberworths, London
.lir Pollution Technology, Painter D. E. , Reston
Fublishrjn,; Co.
Effluent. Tre.rtment in Pr-occs.s tndudtries,
fnst. of Chem. Engg
Eff Iu:n. Treatr-n:nt and I{ast: dj-sposal,
fnst. of Chern. hgq.
Eff luent tre.etment and disposal ,
,'' o.
fnst. of Chem. Engg.
fndustrial
,
Chemistry- Practical- f
Simple Laborltory t:chniques- CrvstaliZei-jsp,
Dj-stj.1laticn,
fractional crystallizrtion,
boi-ling ooint di rgram
fraqti-cnaI distillation,
Extraction process - Phase di:lgram, p,lrtlLion
coef€icient
10
e->-or-
e:<pts
Preplr,ltion of stanC.:rd solutions-Primrr.l ,-.nC
Seccndary stan.lards. Determination of H2 SO4 and
H3 PO4 in a mlxture
8 expts
C,e1i-brrticn of th,:rnor-netcres
2
icquintance r,rith s.lf :ty measures j-n a labor3tor:'
:l .rr: .alL; :? '-h,r.aric-. Is
4 exnl-s
cx-:.1:.
D::termination of physicrl constrnts- Rcfr.ective inCex, 3.:;1,*.,,
surfaee tension, (Effect of surf.eetants on surface
Tension, viscosity- Elui:ls, oolrTmer soluti-ons, ,-=ff :ct of
adCitives cn visccsity, cDtical rotation.
Contd..7.
.
ll
a
a
a
o
l-
3 :xpts
lo;- of s:i:ct ,I cra?-'ni..': ccm:'linds s'rch -.s
:mu-l-nilcrDhcr-;I,f::rlt:'-'l'hfi-/lc'ton:/')Illcos'3/
Estimetion cf f oI ,c.,vlng f ,tirctionrl qrfrlps ir+yt"-lif /, :ster,
acids aminc/ nitro.
S-larrtlon and nrrrif i:.-,tj-cn cf bin-rr-r mi-xturls of tvl'l:w1t- lr
-:,' wet'-lr instl I ubls-wat jr insoLrr";l -'
S,)'l .1DI;l-w-t3r insciubl
Iiquid-sol-id, ,.rfl1 li?r:id-liq'11-; exp:rin--nts bts:"r oa Dr-lnci"I -'r
.:
of I I;,-ctroch.rmistrrr -iDolic.ti-:n cf phls: r-:.tl:: tl si':,o !
-l':r'rrrct
rnrrlticon56!!enL syst-:m, D:t:i''rLin-.1-iDn ':f soli'rbr-i-i--.'
sinrl-e ,.:I:ctron pot:ntial incl'l'!-in:l oct:ntio m t::ic
cf cguivT l:rrt- :r-'ir'))'-'-':c' - cf si-rcn'l ::rd w'-''-k
d=t:rrnin-rticn
,\j
:I rct|I,,rt :s D.atermln:tion' of ils:;-:'s; -'tlJn ''lrn:c.rnt
6( l+t' t
A
15Ii;-:-+-, rtircel s.- ci
usinq PH rn,:t:r.
Esf-r'i rh;'-L
')'-'-rs')n "L rn'-ir tim :rli'e cornput -'--'
Srrs'J .-,'rs. Js_r of vlorr] 'prt' lils)rs/
C,:rnputer lcnIic,.-,ti:ns : us: :f
anl oo:r.rtj-nq
intrrlctinq
'Lf 'lic'- --it''lrns i-'to C ':n'J Fortfr-n
gp,f':::id sh,:r:tsr Tr:nsI':ticn
I.rnqr:'rq'-.LIseofrn'rch:nltical-ndstrListlc-rls'rfLw-r:
p.ci-'11,s,D:mcnstrrti'-':-t:'-:<r-:+''i-l-lcfmcl:ci;'IlrIro'f:Il-inrr
! ? i q)i)
an,J nol lcu.I ir gr-roh-i-c s.
!
Li+
a
Dimensions and units
; lasic Che'ni:a I
Calculat j-ons ltomic weight, rro-lecular wei
tht,
(:
..trs
)
equi'.,aIent rueiqht, moIe, Comros-r_tj.cn of _
(i ) liquicl mi.xtures, and (ii. ) ga.seolrs
mixtures
Matcrial Balance -^rithout Chenical Re:ctions
Flow 'iiagram for naterial_ b:Iance, sirnple
material balOnee witir or withcut r.ecyct: cr
by-pags fcr chernical enlinee::ing coer.-a..ions
such as ci stirration,
absorrction, crrrstai r-iz;rt i.cn,
eva5iration/ extracti_on, etc.
Material Balance involvin.l Chemical R..,,_rct-i)n
Concept of l-in,1tin J re, ctant, ccnyel-.sicn .,Lr.
Id,
,
Liquid ohase re.lction , 1js Drjase reactions,
with,/wlthout recvcle or bv-t-, rs_e.
(
an.l FIui
_
f
l_o,nr
rrrs
(rs
Hrs)
(rs
Hrs)
ind hee,- tr.,r:.rtf,ort
Util i tic-s in Chemical Inlusr-;_.y
Fuel - 'jV.tes of firel_s _ .i.iv._-ntaq;:s ,.rnrl .lisalv,_:.ntaqes
combr:stion of fuel_s, cal-orific v;rl,re. Specificttions
for .:-',_lel oif
Boilers r,{ate-i:
T\,roes
of boil-ers and their functioni;r.1
- Specifications for industriaf use, variorrs
water- tr:eatrnents.
Steam - Genereticn an.1 Use
.Air
Fluid
Soec-i
f ica*.ions for industr_ial use/ Drccessinq
cf 'air.
Fans, blowers, ijornDr:essor.s.
veC:i,rr1 punDs, ej ectcr
Punps : R.eciproc++-ing :- - _a lcar DumDs,
Centrifugal -rumps
Heat Tl:ansfer :'Heat Exch.rl,l:trq ._ Shell- anC
lube
ty:e.. finnec tu.be heat exr:j,ranqers, nlate he:_t
e--(CI1-nq-aps, refriqeraticl
cyc i_cs
)
(tt Hrs)
Ener'ry Balance - iJeat C.:-r,i r,; i i:z
-): ,Jr-jr-(1 arase3 3a,f
gasecus nixtures ,et constant pr.2ssr_rr.:s. 3ensi;:_Le
hea; cha.nr-res i-n iiquids, Ent_aal:.r .llt.,, narcs
Utir ities
l)
I lo'u:
(4 Hrs)
(,+ urs
)
(t
)
urs
ContC. " 9.
.
tt-
-9BOOKS
-stoichiometry, B=r.: Bhatt and s_ptvora
Tata Mccraw-Hi_l_I pubLishlng Company
Ltd,
Nerar
Delhi
Chemica] process princi,ta-l-s._ part
oocr
o-A- Hougren, K-M- '[atson, R_A_
Ragatz
,lsia publishinq House,
Bombay
fntroductj_on to Chernlcal Enqineering,
'I-L- Badger anrt
J-T_ Banbhero
;:cGraw-Hill Bcok Co_ U.-S-A_
tinj-t operations in (tremicalEnqineerinq
''r- L- Itctabe anrf J_C_ ,tnith
l,lcGra',s-Hi1l- Aook Companq, New york
I
Chernic.l Enqineers , Handbock
, -H- ..erry, i{ccraw_Hill
Book Co_,
New y-ork
Operati,)ns _ f and fI D-.D_.
K+1e
Dune ViCyarthi Griha prakashan, pune
Tj'r-r_it
Standard Hanrlbook of p-Iant Enqineerinq
Editorsi
R-C- Rosaler and J_O_ Rlce McGraw
HiIl- Book Co.,
}lew york
u%
Mechanical. properties of
materials anrJ chanqe
vrith resDect to tennperature.
tlaterials of constructions
used
l^
\ z l-il
in fndusgry
(
1.,-ro,cercres anC
.
-s
a
rlr:-:
Lheir applicaticjns.
(+ Fl ,.:'
(+ ts "s)
Contd.
t j,
,
\\
t'
-10
lz-
-
Polymer-ic materials: In,-ius' rial
ccrncosi-te ra.rterials -
colyrner
an-1
(o urs)
Therr constit:ttil-r,
Che'."r-i.ca1 anC phys;ical
properr-ies, InCr:strial ap:li-eations.
ass T\/pes, cornpcslt ion, ilanuf actul:e,
ohirs' cal and Chemic.rI'troper"-ies,'iprllicatlons.
(+ Hrs)
Gl
corrosion - varilus tv'roes cf corrosion rerevant
(+ Hrs)
to chenrlcal industry - Mechanism, Preventirre met'iccls.
Dist.illatlon
distillati.on,
fntroducticn; tsatch and ccni- in'.:.ous
Separation of azeot.:cDes, )l.lLe
(g nrs)
col-umns anC packed columns.
Alcsorotion fntroducticn ; Tquir:il,,:nts - p.lcked
cclumns, sDray colrrr-nns, ):Lt.-:>le crL iumns I o;:.:k-e-1
bubl:Ie colu"nns, mechanicallv a:;itar:e'1 contractcrs.
(g Hrs)
EvapcratiDn fntroluction;
Equipllents - sh,:rt.
trr'ce ( standard ) evaporstor f orce:l circrll..- -'-i.tri
cveDorators, fallin^.r fiI.n evaoorrtors, c1i_moing
fil r (uicwarf flow) evapo-:.itcrs t '.ti':.:') (aritat-=C)
f ii -i evaporatcr.
(e Hrs)
Fil-r-retic:-l Inr-rc:lucti_on; FiIter,ne.lia and
(a r{rs)
fif :ei- alils, Equj-oments - r.Late and frarne
filter pres.s, nutch filter, rotary drum filter,
slcarkler fil-ter, canCle filtef, bag filter, centrifuqe.
Cr,"/3ta1Ii-zation - fntrorfuctl,:n : solrrbiltty,
(e F{rs )
.crvstcl,lrcwth,'
su:ersatrrration, nuc.Ieati on,
Eqrrinment tank crystalLj-zer, arit.ltel
cr./stall izer, evaDor-ator crystall-L zer , ).t aiL
tube cr:y.stallizer.
(s itrs)
Ext:-actiorr f ;rtroCuct j-on: se jectocn of
sol--zents; EqriOments - Sprarz co.Ir:.mn, :ac<e'L
columll. rotatinr^r'1iq: coIu,,,r,. mizer-setti.::-.
Mixinq - fntrocluctioni nixln-y of liquidlliquii,
solid-soIj-o, Iiq,riil-soli I systems.
- fntroCuctlorr; !'ree .lo.t_sture, bound
moisture, drying :urve; Eo,-riprnents - tray dr-ier,
Dry-rn."1
(s
(
Hrs)
s t-trs )
Contd..11...
)'
!t
{
t
.
-13-
-11-
rotary dryerl' ' flash ,]ry=t, fluid fsrC drrzer, drum
dr'y'er, s lray .4J !nrsr u! .
'1
300K3
Science of Ceramics Chemlcal 'orocessing,
Hea:h, L-LChemistrlr and Physics of Cl-avs otner ceramics
,Scj-ence
of ceramlcs, Stewart, G-H-
Cher.istry of eenert
Pr:',erties
of qlass, MoreY,
G:l,tI-
(lh.:-:,tj-stry of qlasses, P:ul, A-
Corr-osion : Causes ,rn,.i. prevention, Spellur, F-IT-
Corrcsia': enli1?!r1i1 lr
Fontana. Ivl-G- ani Green N-D-, Mc Gr i"r-llj--i I 3ock co'
Corroston
an,.l-
Experiments in Material-'.. Teclrnolo.r.r, a Laboratory
Text fc,r Enqineers, }{an.-if.-.;..ri-,ir.: lretaIlurtry. and
n3tcjals te-sCj,n1, 'Sovt. of fnCia; :asr-- 'vcst'
pubiication.
Selectinq Materials for Proc=ss Equiornent
Mc Ma,:lhton :(-,f-, Mc Graw - HilI Bcok co'
fntroCuction tc Chemical Enqineerinrl,
,il-T,- 'iar]rer anC J-T- Banchero
iulcGraw-.HiII aOok co. '.I-s-AUnit o'oer-ations in Chemical Engineerinq
'rf-L- I{ccabe and J-C- 'tnith
Mccr:aw-itill- Book ComparrYr New York
N,'>)
d* [
r
rlana'ie'Lent -ir I:liustry;
I,'j,,ctions cf i-l:^irli{€1icl]tr'fecision :llk.ing.'
Cor^cept of scientifi-c
(4 Hrs )
(9 Hrs)
Cont.l. .72..
\s
-. ll*
_72_
p-l.anninq, organisinq,
Ci -ectinl
.rnd ccntrof
,.
Locat-ion of InCustry,.
Material s
(: srs)
man,.lqe:nent,
(
fnventory control;
s i-ir:-s )
(+ urs )
Manaqer-nent
of hur-nan resources_selection,
lncentives r4slfs5g and safety.
(:
Hrs i
Process in strunentation
Concept of neasurenent anC
oCCurctcy
Princicle'
mea.surinq
construction anc wos(irr.- o-l
fcr
i_n
strument s
(z rbs )
rornrino
Temperature - glass therrnometers,
:i,_reL tlI_ic
therrno.neter pressur-e sprtnq
therm.6r_1r11,11. r/i:r_.ro-r
fill ed thermometers resistance
ther_rc.net=r.s"
radi..:tion Dyrometers
Pressure, _ j,4anometers,
baro?nlter-s, bourrlopressr-tre gauqe,. be1lo-.nr type,
diaci:r.?m type
pres.erlre gauqes, rn:rcleod geu?es,
Dirani_ rrarrr-yoq
I s
etc.
(lo
(t
Frrs)
urs
'vr"'
crcce:luresr slirlpfinq of brrlks
materials, (: Hrs)
?echn-iqtres of sam:Iin1
solirls, liquids and ,Jas€js
collectinq an.j orccess_in: cf
date
(z Hrs)
Chrr:;'ratoqraphy, p,_rp er c hr.Jina
to qra.ohy,
\,' HfSZ
TLC, ]LC, I]PLC
Particle size .leterrnj_nation
(z Hrs )
Rheol ogical i:rooerties of l
iqui.i s, cl.estics and (: Ai-s)
the-''-r analysls
Samp_Iinry
Moden, instrl-rmental_ nethoCs
of an,ll=,/sl-s
UV-YI sil:l e soectro so)l/
fR-s)ec+iI'OsCopy anC nOn-cliS.r=-rSiVe
fR
Nl,lR-.srectrosc6py
Itomic,'ibscrotion, tr,1-ax:o :fhoto,letnr
Neutron liffracticn
a-ray florescenc=
fon-selective el_-ctrodes
'
.
.(: Hrs )
(3 Hrs)
(: ttrs)
(3i Frrs)
.(-L .drs)
(r Hrs)
(r Hrs)
(r urs)
Contd..13.
)
*,
a
(;
-1 3-
fon' chromatoqraphy
Li;-Li f I ev el : Dlrect
in.ijrgsl liquici -l_evel
meisure"nent, irl_oat type liquid level- ?auqe,
ult-:asonic Ievel_ gauqes; br_rbbl_er system
(e urs)
Denlity measurement
(z ars)
-,ri
:r:csity
me.f
surement
(r
'
Hrs)
(2 Hrs)
BOO.(
fnrl'tstrial- Orqanizatioi-r a.nrl nan.lqement, .Bethel
fnd strial- instrrrment lticn
-'J.P, Ec]<.nan, Jchn-wileys & Sons
,l,cniied fnstru.nentati_on in orocess fnrlr.rstrles,
iicl . I, fI & Iff W.G. -\ndrews, Gulf :un]_lceticn
L_L_
sLrtrrmentati:n :nd Ccntrol f:r t:re proccss
industries, S. Borer, Elsevier Jp:lied Sci=nce Dublishgrs.
Che:rric, I rjnqineers, an.rl boc,t. J.H. De:r:ry and
D ,-1.'eenb, Mccgraw-Fli1l lcublishinq co. , Nqw vork.
fri
rnscruirtentaf meth.l.ts of chemical analysis,
rvi-11arr... ].,i..-^rrj_t, )ean, Sett_.:l
rntrrduction tc 1.-str':mental analrr..sis, Braun R.D.,
iic ']raw. IJil-i phblisL-ring co.
Rhecl
ogy Theorv ancl ap.:Iieation., \r-Oi. 5, Ff.rieh, R.; !-inal -rtical Chemistry, ,T. G. Dick, I',IcGl .:.w, Hi I l_ Prrbl ic ation Co
rnt itatlve fnor.Janic,\n:,Iysi s, .\. -,,rogei, Lrn6r:n ?ublication.
fr:strumental i"lethorls cf inalysj-.s, SKolq an.J -,rest.
rJr.-l
lr"\
uni: Process i;i one to tr,rro examples cf each of tne foil0wing
unit ,f r'l(resses
t:-'-i-cn, su.I rhcnar-ion, Friecel- craf ts reacticn, 1c
ex,ots
este;i f i c it_icn, l{yCr:l.rsis, oxidaticn, Hal_oqenaticn,
chroi:o: rlphcn:tion, Reicrctirn, polvmerlzat.Lln,
reclCticns oE Ciazc:-irun s.r .l_ts
process rnrtrurrentation- tr':,r.ns,lueers of rlifferent types.
use lf Transduc,)r's fcr '12.-",tring florv control
10 ex,ots
Detenni iation of fl-ash n:_.i-n .in-l ioaition r::ints of riquirls
lfatcr analysi s- so I id eclteirt, H.trrlne:: s,
1C expls
Ni
Cnnt I
1
4-
\
rt
-
16',*.
-L.'*
coD/ and other tests as per industri-al spccri-ficrlions
Fl-o,,v measurinq Cevi-ces"fcats
Monoqraphs of. reoresentative rf.w materiars
15 expts
such as sr:lphurlc acid, tcluen=, sodium, carboria.te,
scdj-un hyroxlde, carbon terachlorrrle Benzodc.r acid (5-6 compouncls)
Limit tests for heavy metals Pb, .lrsz Hq, Fe ;n.l esh content.
fnstrumental .rlethoCs of analysis
15 expts.
1. Soectroinetric / cqlclrcimetere rfet=rminatron of GJ-uccse,
Y-.-xture of 1) cr+Mn (z\ Ti+v
Flame photomeric detr:rmination : Na, K, Ca anC Li
Ion exchanqe sep.sration separar--ion of Zn*l'In, en:1 N:-+Co
TuroiConetry : Determination of So2
: Deterrnination of copDer
Electroqravimetry
Pclarogranhy
i:; Determination of cc ..nd Pb
::: Determination of Pb in Pb+Bamixture
CoUlometry
impe;:cmetry
.ii Deterrnination of 'Pblga rrith l€
k.rcr
o+
l::I.l:::::,:':i::::1"",,; ;":,:i:":,": :: ;:#"llil;
Ccnductometric titr.ations:ti
fnCBstrj-al-
Chemi
stry_
H,r.q*
Mixture of acetic acid mono chloro
and trichLoro acetlc acid with
NaOFI fr :erpretatj-on of ETf R, NIUIR
and i,lass spetra.
-__.P_aesr V
Ch?irLLcaI Process Econo.nics
Factcrs involved in oroject cost estirnritlon,
Methorls enployed for the estimation of capit':Jinvestment.
(O grs)
Caoital formation- Elements of cost accounti,-rq.
(S ilrs)
fnterest
r.nrf invest'.:rent. costs, Time .ral-ue of
Monev-equiva I ence.
(: IJrs)
Depreciation, methods of deternining
depreci:ttion/ Taxes"
(+ Urs)
Some asp,ects
of ,n.erk:tj.n,-; fricin,r oolicy.
Prof,itability
crlteria,
al-r-ern at ives.
Econr:rr-nics
o! selectinq
(4 tirs)
(: ttrs)
Contd. .15..
fA
'c
'- l7-
-.15-
V.eriatror of cost with cao .::ity, Break_everr
(S Urs)
point. optimurn brtch srzes, oroduction sche.lulinq, etc.
BOCK
Econornics of Chemical fnCr:strv, Hemcel. E.H.
Unit
l_n
anic Ch:mlst
1.{:ingfaCtrr5.j
-I
I{rtration
: fntroducticn - Nitr,itj_nrr aq.3nL,r,
Kiretics anC nech.tnl-sn of nitration,
?r)ces.j.)s such
.--s n.itr.rtior: of
: i ) Paraf fi-nic hwCroc.rr).rons,
ii)
Benzene to nitrcbenzene an1 m-rfinitrc]oenzerte,
iir)
Chlcrobi:nzene tc o- tnd p- n_it-rochfor-c
.re:r .enes i-'/) \cetalilice
to t:- nitroacet.rni.,-idc:
70 Toluene
(rz
Continuclls \/s batch ri.,r:ati.ln
Ilafo,:en1tion : _r_af r-)i'rction - Kinetics of
halcgollti.-n reacti.r.lq., R,:-:-rent.s fcr
haloq.rn.rtlon, Ha 1-613p1 etion of aro.natics - side
chain -,nd nuclear h.tlor:.:n: tions, Comrercill
rnanuf.':ctr-lr3s - chl-orobenz"nes, chlora},
mcnochlor-ec -:tic -,r,f ehloronethanes,
d ichlorof I :-roromethan e.
Hr-s)
(9 Hrs)
,Su-r.lhonation : Introduction
s,r_lrhonating
locnts, Ch:mical anC chysic.I factcrs in
sulohonaticn, itinetics rni n--chanism of
sulphcn.rtior-tre--rctirn, Commercial suffon.etion of
benzene, naphthalene, :Llkyl-'Jerlzel;ret tsatch
Vs contj-nucr:s sulohon.-Ltion.
(9 urs )
OxiCation : Introduction
T\rp,:s of oxiCa.ticn
reactions, Oxidizing aqents, Itin :i-ics -n.1,
(l
Hrs
)
mechanism ,cf oxid:tic,n of :rqenj-c coinpounrl:
yaoor phasi: oxi--lation,
Conrnercial nrenur-'act,lr= of cenzoic -rci.l rii,-reic
;:plhydr-1de, phthalic =-nhydriCe, acroiein,
ac?tal.lehyde, ac.:tic lci l.
Liqui.J nl:ase oxidatioa,
I'ydroqenation
: fntrodrrr :j_on - Kinetj_cs
thermodynarrlics of hydrogenation reactions,
and
(l
t
rs)
ContC. . 16.
IT
.
1a
__ lg_
t
Catal-vsts f or hyirogr:nrtt-cn r: rctions.
Hvdrcq:rration of ;egetai:I:: --'-L, ii'-inufacture
of rn:thanol frcm c'rbon rncnoxide anf jrydrog2n,
hydrogenatlon of aci'is and -:sters to algohols,
cata l-ytic ref orrning.
(l urs )
: Intro.luctlon; TVpes of alk1'Iation,
a?ents, Thermodynamics a.nd mechanisrn
^lkyl-rting
of alkyr-:tion r:act.ions, Manufa.cture of-alkyl
benzane.s (for Cetergent nanuf acture), ethyl
benzene, phenyl ethyl alcohol, N-alkvl aniLin':s
(mone anl Ci-methyl and ethyl anil-ines)
^rlkylrticn
: fntr:o'luction,' H-y:1roCvn.''nics a-:rJ
Esterj-fication
rercti:ils,
kie:tics of esterific:tion
by orqanic acir'l-s' ':r'7 ril'iit . -rn of
Estcrification
rlnsaturate$ comnounds, e'sterif icltlon of c:rbo>q7lic
aciil deriyaives, corrln rrcirl ',1:auf -'-.-)r ': cf -t-:thyI
acet.ate.rl6cty] Dhth;llate/ vinrll 1c'.'-rr-e/ cel-Iul-o'se
aC
er-et
".
(l
: rnt-roducti:n,
-\min,,t.1o-r : (a) ey r:ductic--i
lvletl"cds of reductioD-rl ,-t?-l- lnC lciC, c-talytic,
sul5r.1e, el.,--ctrolviic, 'n::t'I and all<rIi sulf it:s,
metai hydrj-c1es, sodiu,n metal/ concentrated
eaustr-c cxldation, r.-duction, comrnercial
Hrs )
of lniline, m-nitroaniline, p-:mino
ph,:rr.>i b) tsy aminolysis : fntrorluctj-on, amin'rtjnq aqents,
manuf.-.ct,,-tre
f
^c
i-ci-s,ef f ect-lnq,
Hydrcl.gsis: fntroduction; hvdrolyzing agents,
Kinetics, thernodynamics ancL mecha-nlsm o€ hvdrolvsis
(Z i{rs)
tsOOKS
Unit, rrocesses in Orqanic Synthesis,
McGraw- HilI gook Co., New York
P.
Fi- Croggins,
Contd. .17..
.
t,ii
t
'
:,t
:
t
:
i t"
^r
l
i''iil':-.'j,''
Hj-stor:ica1 b.tckcrrc::l-l aail ,lev,:lo:.n,:nL f ,i.rl "- ,i.:eut.ical
:' i
i
i' " ''
.irr '-Tnl:i-.. ' r :rl:ll.f .:f .
'
tndustrryi
'.
:J
,ril .
';
2L
i-j1,.
,-
Pharri:.cdpoei'rs -,.., r, -:,:r.-,redt .c-'f TnCi, n p..1.rr- ,c r*)oeia .l,.c]
intrcc rcti,ra'tl :,t i i'l ii.',i-.,t iT.p. ; Y.t. nn,., ;-,. :l:=r'i-i-:''i'
2L
3L
.:iltJ_u(1.1_s--J_rrEnr(]uct'L2n t,o pliint
-i.t-';r i .j:( i.-'' ,:li-. -,..'-r. -l:..:'
. col_l
ruqs,. c rl- i-i.z-,.8-Lon,
fof
=ctionr pr=r:ar.riion
-:-.'
''
_tne
:i ":
' -:.1i' '-i
nSa:stor.fe.? , cf m:l-l j Cin:.!' .to1 rnt,s.
t:,,,f rLr-.1 ,: ,i,,, .:,1. 11-i(. ll?.r. .rc:li?.ri-',.'r1l'..-J-;,Ej f1:--ii,'b;. IOln
qar.
,l
eJ..1sgj,J; ..taLion^,__r.Rd 3L
Evaluation of crurie cr-uqs - i{oi-sturi: cont.ent ..:xttraQt.iirc'
lE.riJfrlE, volatile o.r,- content, _ fgr;iqn o6g:rnic,,ritter.. .
-il'
i:' "- :'! l''"';'..
' 'r'
ex ercl.ses, includ-in? of starch,
Quantitative micros:o:ic
, l-eaf cOn|-ent (palis,r.ie :r rti6ri Sto.rn=taI numbS::, r,nd: f6,fEx
AL
,
slet nprlbeE i;nd vein. .t,:pqrina!ion.riurnbe,:- r enude ;f,,i]:re
eontent. introducti.tn Lo chromrtographie ,:net:-^rc.I:.,r'tr i ', r..;
. ' ,. vein,.. i
j-dentification
of ciude Crugs.
Ghemicbr constitur..ion .r,' ;)rarits - rnc1u.lin- 6' :t,rhrydr.1tes, 9L
amino. ..clds, protel;,5, f at-s. .,'['.:xes, vol ri-llll i :-sr;
r
terpenoids, st :rior:trs,,:.
s;-rpo;tins,,- f.kavonol.r]s,
g11rcoside,s,-:l-k.:1oi..ls.: o
.,i,
.:
,
t
1:rihsi,
.
:,
3L
6L
pyroerenic t =;t : nq, qL s s t :st- irro, butrk
*$ - *. .i
den.s
it', of
Introducti-on tc v--r.rious tyn,:s of formul,-rtions rnd roots of
' ,admiri straticn.
,\septj-c conditions', ner=j fttr
of steri-lisation.
2L
.t
rnetho.l s 2L
st :r1i ; at iori, v :^r'-c'.:s
Varlorrs tvrcs of )nlrm3ceutic.rl- cxcipj-ents -th:ir
l2L
chemistrye process cf n'rnufacturc and gualitv,
specj-fj-cations Glidants, lubri,clnts, dilu=nf :, -'f,resi:rv^tiv=s,
antioxiC':nts, emulsifyitz .l.li3nts, coatinq aqen'Ls.. llinCers,
|
-1.
\
-
i--,
i
'
,
f
.
-2rAI
colorinq 3q,:nts. Fl:vourin<: ,.r.^fr:nts, q:1.:tin rnd other
addj-tives, sorbito j , 'n:nnito r \rj-scosity brril l.-:rs, etc.
.
Surgi-ca1 dr-:s.si_n.Is 5r11r.11:-5; liqatu.es-
r -3Dect to
the process, :qui:':::flts ,rs lrj frr n,^nufactur-:, ir:thod of
sterllzation anC q','iIrtr/ contrcl.
r..ri,-_h
Pharmac,:ut.ic.'1 D-c :' -i.t- - fntro.luction,,l,1cK-_
selection, packaqir:.: mrter:ie1s, ancill_:try rn,.,t.:i-i-,-r1s,
5Ir
5L
packaqino "n.:lchinerv. eualir_-,r control of p,-ckrrinq
m.eteri
el-
s.
crassif icetion of -r-.rlcus tyo,:s of druqs ,vith examples .
i_2L
materi,als, process of manuf.tcture, efflUent handling,
etc, of the fol-lowing bulk druqs
(f ) Sulph.a drugs &r1oh-,q..rrnd1yl_-, sploh-.p*[email protected]
Raw
(li)
lntlmicrobial - ehlorr-lph,5ni-e y\. furezoliWind'
mercurochrome, isonlazld, N1-Pi'Sr
(iir) .1ntalgesic-entinf lamrnatorv - salicvlS ,"i,f :nc its
derivatives, Iuprofen, m:fen;rmiE,TiC.
(iV) Steroidal- hormones'- nroqist=tl?=, Testost.rfine,
methyl testost?rore.
tv) Vltamins - trit. .-r, Vit.B6, vlt.C
(vi) Barbi-turttes - Pentob,:rhital
(vii) -BJockers - Propr:no1ol, ?.t,jnol01
(Viii) Cardiovasculrr rg,3nt - Methyl dop.e
(iX) -intihistarnines Chloronh=nerami_ne mtle= | -:.
Products l:ased on fernontrtion proc"ssesBfj-etr idea of microorg-.,nisins, their struct,ure, qrchrEh
u.refulness. Enzyne sirstens useful for trrnsform.rtion,
mierobj-al, produets.
General prlnciple of fern3ntrtion
proeesslnq.
PTOCCSSGS
t2L
1nd
rnd croduct
\], -
l,Ianufagture of .rntiniotics - . enicillin
- c and
RiE-,1mrrcin, tetracyelins, .,/it. ts L2
't\
Blotransformation processeS - fer
, 1l
* Ere,tnisolone
-$;
hydt'o>orlation in steroids..
' I r$:
semiqvnthetic penicllIins,
Enzyme
t'
c
o-
-18-
ei_alyzad tr.ensformatio
Retero synthetic an-_rlysis c,-lnd
nloleouJes { Se},':c.t.eo from vLta
Contd.ll %.
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